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Beilstein J. Org. Chem. 2015, 11, 2267–2277, doi:10.3762/bjoc.11.247
Graphical Abstract
Scheme 1: Schematic description of self-assembly of γ-CDs with PMA-PPO-PEO-PPO-PMA and one-pot endcapping via...
Scheme 2: Synthetic pathway of PMA-PPO-PEO-PPO-PMA.
Figure 1: Photographs of the formation of a PEP100M15CD hydrogel.
Figure 2: WXRD patterns of γ-CD (A), PEP15CD (B), PEP100M (C), PEP100M10CD (D), PEP100M15CD (E), PEP100M30CD ...
Figure 3: 1H NMR spectra of PR30CD80P in DMF-d7/D2O (A) and DMSO-d6/D2O (B).
Figure 4: GPC curves of γ-CD (A), PR0CD30P (B), PR30CD30P (C), PR30CD50P (D) and PR30CD80P (E).
Figure 5: 13C CP/MAS NMR spectra of PEP100M15CD (A) and γ-CD (B).
Figure 6: 2D NOESY NMR spectrum of PR30CD80P in DMSO-d6/D2O.
Figure 7: FTIR spectra of PEP100M (A), PEP100M15CD (B), PR0CD30P (C), PR30CD80P (D) and γ-CD (E).
Figure 8: TGA curves of PEP100M (A), γ-CD (B), PEP15CD (C), PEP100M10CD (D), PEP100M15CD (E) and PEP100M30CD ...
Figure 9: BrPEPBr (A), PEP15CD (B), PEP100M (C), PEP100M15CD (D), PR0CD30P (E), PR30CD50P (F), PR30CD80P (G) ...
Beilstein J. Org. Chem. 2010, 6, No. 37, doi:10.3762/bjoc.6.37
Figure 1: Boronolide (1), boronolide analogues 2–3 and gem-difluoromethylenated analogues 4–7.
Scheme 1: Retrosynthetic analysis of target molecules 4–7.
Scheme 2: Synthesis of target molecules 4–5.
Scheme 3: Synthesis of target molecules 6–7.